Troubleshooting
Improve your analytical sample preparation skills with expert guidance on troubleshooting common issues. Identify and resolve problems in liquid/liquid extraction (LLE), Soxhlet extraction, QuEChERS, solidphase extraction (SPE), and filtration to ensure accurate, reproducible results. Learn to overcome challenges like low recoveries, sample contamination, emulsion formation, clogging, and poor extraction efficiency. Understand how solvent selection, pH control, and sample matrix effects impact performance. Our interactive learning content, expert knowledge, and troubleshooting insights provide practical solutions for optimizing sample preparation in pharmaceutical, food safety, environmental, and forensic analysis. Start learning today to enhance efficiency, minimize errors, and achieve high-quality analytical results.
SPE - Troubleshooting Recovery Problems
This short video details how to determine if you have a recovery problem and defines step by step procedures which can be used to assess at which point in the SPE process loss of analyte(s) is occurring.
Investigating SPE Recovery Problems
This quick guide details how to determine if you have a recovery problem and defines step by step procedures which can be used to assess at which point in the SPE process loss of analyte(s) is occurring.
Troubleshooting SPE Reproducibility Problems
The first step in troubleshooting irreproducibility is to verify that the analytical system is functioning correctly. Reproducibility problems can be caused by sample-to-sample carryover, detector problems, or a defective autosampler. This article describes how to troubleshoot these problems.
Troubleshooting SPE Cleanliness
Previously we have looked at troubleshooting and resolving the problems of poor recovery and reproducibility in solid phase extraction (SPE). Another common problem we see with SPE is poor cleanliness which will be the subject of this article.
Troubleshooting Liquid/Liquid Extraction
This quick guide details how to troubleshoot the most common problems encountered in liquid/liquid extraction techniques.
Troubleshooting Filtration
This article will look at selecting the correct syringe filter, where to find relevant information on selecting a syringe filter, and what common problems may arise during filtration using syringe filters.
Troubleshooting Sample Preparation: Filtration, LLE, SLE, and SPE
This webcast will look at some of the most common sample preparation techniques and discuss how to select the appropriate one for you. We will then discuss what can go wrong during sample preparation and how you can either avoid these issues in the future or how to remedy them if they appear.
Troubleshooting Sample Preparation
This webcast will address some of the most common problems encountered in the lab when carrying out sample preparation using filtration, liquid/liquid extraction (LLE), and solid phase extraction (SPE). We will provide troubleshooting strategies as well as tips and tricks to avoid problems in the first place.