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The first step in troubleshooting irreproducibility is to verify that the analytical system is functioning correctly. Reproducibility problems can be caused by sample-to-sample carryover, detector problems, or a defective autosampler. This article describes how to troubleshoot these problems.

This quick guide was written by Dr. Dawn Watson (CHROMacademy Technical Expert, Crawford Scientific).

Troubleshooting SPE Reproducibility Problems